1KPB
PKCI-1-APO
Experimental procedure
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X4A |
Synchrotron site | NSLS |
Beamline | X4A |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 1995-10-19 |
Detector | FUJI |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.110, 77.290, 81.030 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.000 |
R-factor | 0.187 |
Rwork | 0.187 |
R-free | 0.24800 |
RMSD bond length | 0.013 |
RMSD bond angle | 25.069 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.042 |
Total number of observations | 99583 * |
Number of reflections | 17662 |
Completeness [%] | 89.7 |
Redundancy | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6.5 * | 20 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG8000 | 13-18 (%) | |
2 | 1 | reservoir | sodium cacodylate | 100 (mM) | |
3 | 1 | drop | apo-PKCI-1 | 10 (mg/ml) |