1KIR

FV MUTANT Y(A 50)S (VL DOMAIN) OF MOUSE MONOCLONAL ANTIBODY D1.3 COMPLEXED WITH HEN EGG WHITE LYSOZYME

Experimental procedure

Detector technology	AREA DETECTOR
Collection date	1994-04-08
Detector	SIEMENS
Spacegroup name	C 1 2 1
Unit cell lengths	129.220, 60.450, 56.770
Unit cell angles	90.00, 119.02, 90.00

Refinement procedure

Resolution	7.000 - 2.000
R-factor	0.167
Rwork	0.167
RMSD bond length	0.016
RMSD bond angle	1.910 *
Data reduction software	XENGEN
Data scaling software	XENGEN
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall
Rmerge	0.082
Total number of observations	47313 *
Number of reflections	21066
Completeness [%]	82.8
Redundancy	2.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *			used to seeding *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG8000	15-18 (%(w/v))
2	1	reservoir	potassium phosphate	0.1 (M)