1KBG
MHC Class I H-2KB Presented Glycopeptide RGY8-6H-GAL2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 133 |
Detector technology | IMAGE PLATE |
Collection date | 1996-02-01 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 135.870, 86.840, 44.980 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 18.000 - 2.200 |
R-factor | 0.224 |
Rwork | 0.224 |
R-free | 0.27900 |
Structure solution method | MR |
Starting model (for MR) | 2vaa |
RMSD bond length | 0.008 |
RMSD bond angle | 1.400 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.170 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.078 * | 0.384 * |
Number of reflections | 28511 | 1734 * |
<I/σ(I)> | 16.2 | 1.9 |
Completeness [%] | 89.3 | 55 |
Redundancy | 5.4 | 1.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6.4 | 2.3M Na/K PHOSPHATE, 2% MPD, pH 6.4 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | protein | 18 (mg/ml) | |
2 | 1 | 1 | sodium potassium phosphate | 2.3 (M) | |
3 | 1 | 1 | MPD | 2 (%) |