1K7G
PrtC from Erwinia chrysanthemi
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 1999-03-01 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 101.892, 101.892, 122.009 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.000 - 2.000 |
R-factor | 0.199 |
Rwork | 0.195 |
R-free | 0.21460 * |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1kap |
RMSD bond length | 0.004 * |
RMSD bond angle | 1.250 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 * | 2.030 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.084 | 0.494 * |
Total number of observations | 292821 * | |
Number of reflections | 49161 * | |
<I/σ(I)> | 14.8 | 3 |
Completeness [%] | 99.5 | 99.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 6.5 | 20 * | NaCl, pH 6.5, VAPOR DIFFUSION, temperature 293K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | 2 (M) | ||
2 | 1 | reservoir | 0.1 (M) | ||
3 | 1 | reservoir | 0.1 (M) | ||
4 | 1 | reservoir | MES | 0.1 (M) | pH6.5 |