1K22
HUMAN THROMBIN-INHIBITOR COMPLEX
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU300 |
| Temperature [K] | 287 |
| Detector technology | IMAGE PLATE |
| Collection date | 1999-06-15 |
| Detector | RIGAKU RAXIS IV |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 69.370, 71.490, 72.141 |
| Unit cell angles | 90.00, 100.36, 90.00 |
Refinement procedure
| Resolution | 500.000 - 1.930 |
| R-factor | 0.197 |
| Rwork | 0.197 |
| R-free | 0.21400 |
| Structure solution method | OTHER |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.290 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | |
| High resolution limit [Å] | 1.930 | 1.930 |
| Rmerge | 0.054 | 0.298 |
| Number of reflections | 25984 | |
| Completeness [%] | 99.8 | 98.3 |
| Redundancy | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
