1K21
HUMAN THROMBIN-INHIBITOR COMPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 287 |
Detector technology | IMAGE PLATE |
Collection date | 1999-06-15 |
Detector | RIGAKU RAXIS IV |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 69.619, 71.546, 71.821 |
Unit cell angles | 90.00, 100.12, 90.00 |
Refinement procedure
Resolution | 500.000 - 1.860 |
R-factor | 0.216 |
Rwork | 0.216 |
R-free | 0.25600 |
Structure solution method | OTHER |
RMSD bond length | 0.007 |
RMSD bond angle | 1.790 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | |
High resolution limit [Å] | 1.860 | 1.860 |
Rmerge | 0.054 | 0.251 |
Number of reflections | 28635 | |
Completeness [%] | 97.7 | 94.3 |
Redundancy | 7.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |