1JZT
Crystal structure of yeast ynu0, YNL200c
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X12C |
Synchrotron site | NSLS |
Beamline | X12C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2001-05-16 |
Detector | BRANDEIS - B1 |
Wavelength(s) | 0.9788, 0.9785, 0.9400 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 57.732, 68.676, 125.187 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.260 - 1.940 |
R-factor | 0.2 |
Rwork | 0.200 |
R-free | 0.23700 |
Structure solution method | MAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.200 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.970 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.062 | 0.417 |
Number of reflections | 39366 | |
<I/σ(I)> | 12.6 | 5.8 |
Completeness [%] | 98.2 | 92.3 |
Redundancy | 11 | 9.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 277 | ammonium formate, PEG 3350, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |