1JYB
Crystal structure of Rubrerythrin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | CONVENTIONAL Cu |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 1999-03-01 |
Detector | MARRESEARCH |
Wavelength(s) | 1.5418 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 49.670, 81.552, 99.754 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.200 |
Rwork | 0.182 |
R-free | 0.23100 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.017 |
RMSD bond angle | 2.800 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 15.000 * | 2.390 |
High resolution limit [Å] | 2.000 | 2.220 |
Rmerge | 0.090 | 0.376 |
Number of reflections | 10576 * | |
Completeness [%] | 99.9 * | 100 |
Redundancy | 11.5 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 298 | PEG1500, Tris, pH 7.0, VAPOR DIFFUSION, temperature 298K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 10 (mg/ml) | |
2 | 1 | drop | PEG1500 | 5 (%) | |
3 | 1 | drop | Tris-Cl | 50 (mM) | pH7.0 |
4 | 1 | reservoir | PEG1500 | 10 (%) | |
5 | 1 | reservoir | Tris-Cl | 100 (mM) |