1JXY
CRAMBIN MIXED SEQUENCE FORM AT 220 K. PROTEIN/WATER SUBSTATES
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 220 |
Detector technology | DIFFRACTOMETER |
Collection date | 1990-12-21 |
Detector | RIGAKU AFC-5R |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 40.880, 18.560, 22.410 |
Unit cell angles | 90.00, 90.67, 90.00 |
Refinement procedure
Resolution | 17.670 - 0.890 |
R-factor | 0.145 |
Rwork | 0.145 |
Starting model (for MR) | 1jxx CRAMBIN MIXED FORM AT 200 K. |
RMSD bond length | 0.011 |
RMSD bond angle | 0.032 |
Data reduction software | TEXSAN |
Data scaling software | TEXSAN |
Refinement software | PROLSQ |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 17.670 | 0.910 |
High resolution limit [Å] | 0.890 | 0.890 |
Rmerge | 0.079 | |
Number of reflections | 27080 | |
<I/σ(I)> | 7.7 | 1.8 |
Completeness [%] | 74.7 | 45 |
Redundancy | 1 | 1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 7 | 293 | ethanol, pH 7.00, VAPOR DIFFUSION, SITTING DROP, temperature 293K |