1JTF
Crystal Structure Analysis of VP39-F180W mutant and m7GpppG complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 113 |
Detector technology | CCD |
Collection date | 1999-05-13 |
Detector | SIEMENS |
Wavelength(s) | 1.5418 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 84.245, 67.741, 79.635 |
Unit cell angles | 90.00, 118.11, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.600 |
R-factor | 0.273 |
Rwork | 0.258 |
R-free | 0.27900 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.018 |
RMSD bond angle | 24.460 * |
Data reduction software | SAINT ((SIEMENS)) |
Data scaling software | SAINT ((SIEMENS)) |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.740 |
High resolution limit [Å] | 2.600 | 2.610 |
Rmerge | 0.107 * | |
Number of reflections | 21940 | |
Completeness [%] | 94.1 | 50 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 4.5 | 298 | Hodel, A.E., (1996) Cell(Cambridge,Mass.), 85, 247. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | PEG8000 | 10 (%) | |
2 | 1 | 1 | 0.125 (M) | ||
3 | 1 | 1 | citrate | 0.1 (M) |