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CRYSTAL STRUCTURE OF P14TCL1, AN ONCOGENE PRODUCT INVOLVED IN T-CELL PROLYMPHOCYTIC LEUKEMIA, REVEALS A NOVEL B-BARREL TOPOLOGY
Experimental procedure
Spacegroup name | I 2 2 2 |
Unit cell lengths | 38.897, 82.839, 117.726 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.500 |
R-factor | 0.192 |
Rwork | 0.192 |
R-free | 0.25900 |
RMSD bond length | 0.006 |
RMSD bond angle | 31.000 * |
Phasing software | X-PLOR (3.851) |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 * | |
High resolution limit [Å] | 2.500 * | 2.500 * |
Rmerge | 0.099 * | 0.288 * |
Total number of observations | 60407 * | |
Number of reflections | 6870 * | |
Completeness [%] | 99.4 * | 99.9 * |
Redundancy | 8.8 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 0.2 (mM) | |
2 | 1 | drop | Tris-HCl | 5 (mM) | |
3 | 1 | drop | sodium acetate | 25 (mM) | can be replaced by Succinate |