1JRA
Crystal Structure of Erv2p
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU300 |
Temperature [K] | 120 |
Detector technology | IMAGE PLATE |
Collection date | 2000-11-21 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 53.630, 66.810, 60.380 |
Unit cell angles | 90.00, 91.44, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.000 |
R-factor | 0.196 * |
Rwork | 0.196 |
R-free | 0.23300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1JR8 prior to refinement |
RMSD bond length | 0.008 |
RMSD bond angle | 1.210 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.070 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.082 | 0.461 |
Number of reflections | 28807 | |
<I/σ(I)> | 15.1 | 4.5 |
Completeness [%] | 99.8 * | 98.3 |
Redundancy | 5.3 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.2 | 293 | PEG 8000, sodium cacodylate, magnesium chloride, pH 6.2, VAPOR DIFFUSION, HANGING DROP, temperature 293K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | cacodylic acid | 0.1 (M) | pH6.2 |
2 | 1 | reservoir | 50 (mM) | ||
3 | 1 | reservoir | PEG8000 | 32 (%(w/v)) |