1JP0
NMR Structure of the LP5.1 Hairpin from Bacillus RNase P RNA Refined WITHOUT Residual Dipolar Couplings
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | DRX | 500 | |
| 2 | Varian | INOVA | 600 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 13C-separated-NOESY (Mixing times of 200 and 250 ms) |
| 2 | 1 | 1 | NOESY (Mixing times of 80 and 140 ms) |
| 3 | 1 | 1 | HCCH-TOCSY |
| 4 | 1 | 1 | HCCH-COSY |
| 5 | 1 | 1 | 13C-Hetero-TOCSY |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 5.5 | ambient | 298 |
| 2 | 5.5 | ambient | 277 |
| 3 | 5.5 | ambient | 298 |
| 4 | 5.5 | ambient | 298 |
| 5 | 5.5 | ambient | 277 |
Conformers
| Conformers Calculated Total Number | 100 |
| Conformers Submitted Total Number | 28 |
