1JOB
Crystal Structure of Murine Olfactory Marker Protein in Spacegroup P3121
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X12B |
Synchrotron site | NSLS |
Beamline | X12B |
Temperature [K] | 130 |
Detector technology | CCD |
Collection date | 2000-03-29 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 1.276 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 86.327, 86.327, 71.574 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.000 - 2.400 |
R-factor | 0.234 |
Rwork | 0.234 |
R-free | 0.26400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1f35 |
RMSD bond length | 0.017 |
RMSD bond angle | 1.700 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 11701 | |
<I/σ(I)> | 12.6 | |
Completeness [%] | 94.4 | |
Redundancy | 19.31 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6.5 | 295 | unpublished structure * |