1JK4
DES 1-6 BOVINE NEUROPHYSIN II COMPLEX WITH VASOPRESSIN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 110 |
Detector technology | IMAGE PLATE |
Collection date | 1996-07-01 |
Detector | MARRESEARCH |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 50.900, 50.900, 105.800 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 15.000 - 2.300 |
R-factor | 0.234 |
Rwork | 0.234 |
R-free | 0.29900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2bn2 |
RMSD bond length | 0.010 |
RMSD bond angle | 26.600 * |
Data reduction software | X-GEN |
Data scaling software | X-GEN |
Phasing software | AMoRE |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 999.000 |
High resolution limit [Å] | 2.300 |
Rmerge | 0.058 |
Completeness [%] | 96.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 * | 291 * | Wu, C.K., (1996) Acta Cryst., D52, 946. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 14 (mM) | in water |
2 | 1 | drop | sodium azide | 0.25 (mg/ml) | |
3 | 1 | reservoir | 2.0 (M) | ||
4 | 1 | reservoir | MES | 0.1 (M) | pH6.5 |
5 | 1 | reservoir | sodium/pootassium phosphate | 0.05 (M) |