1JIU
T4 Phage BGT in Complex with Mg2+ : Form I
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2000-02-10 |
Detector | MARRESEARCH |
Wavelength(s) | 0.934 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 69.827, 102.650, 54.871 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.500 |
R-factor | 0.192 * |
Rwork | 0.192 |
R-free | 0.27400 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1qkj |
RMSD bond length | 0.006 |
RMSD bond angle | 1.260 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.590 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.071 | 0.126 |
Total number of observations | 273212 * | |
Number of reflections | 12981 | |
<I/σ(I)> | 15.8 | 12.3 |
Completeness [%] | 90.0 | 77.3 |
Redundancy | 21 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 291 | PEG 4000, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | PEG4000 | 10-11 (%) | |
2 | 1 | drop | Tris-HCl | 100 (mM) | pH7.5 |
3 | 1 | drop | UDP | 1 (mM) | |
4 | 1 | drop | 40 (mM) | ||
5 | 1 | reservoir | PEG4000 | 20-22 (%) |