1JHL

THREE-DIMENSIONAL STRUCTURE OF A HETEROCLITIC ANTIGEN-ANTIBODY CROSS-REACTION COMPLEX

Experimental procedure

Spacegroup name	P 65
Unit cell lengths	57.800, 57.800, 282.100
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	7.000 - 2.400
R-factor	0.214
Rwork	0.214
RMSD bond length	0.020
RMSD bond angle	4.000
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.400 *
Rmerge	0.139 *
Total number of observations	94553 *
Number of reflections	19835 *
Completeness [%]	95.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	8.5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG8000	17.5 (%(w/v))
2	1	reservoir	potassium phosphate	0.1 (M)