1JDY
RABBIT MUSCLE PHOSPHOGLUCOMUTASE
Experimental procedure
Temperature [K] | 289 |
Detector technology | AREA DETECTOR |
Collection date | 1993-01 |
Detector | XUONG-HAMLIN MULTIWIRE |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 174.420, 174.420, 101.120 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.700 |
R-factor | 0.186 |
Rwork | 0.186 |
R-free | 0.24400 |
Structure solution method | MODEL REFINEMENT |
Starting model (for MR) | 3pmg |
RMSD bond length | 0.015 |
RMSD bond angle | 3.140 |
Data reduction software | XDS |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 2.600 |
Rmerge | 0.150 |
Number of reflections | 45891 |
Completeness [%] | 95.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.4 | pH 6.4 |