1JDO
SPERM WHALE MYOGLOBIN (FERROUS, NITRIC OXIDE BOUND)
Experimental procedure
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 295 |
Detector technology | IMAGE PLATE |
Collection date | 1997-02-14 |
Detector | RIGAKU |
Spacegroup name | P 6 |
Unit cell lengths | 91.506, 91.506, 45.853 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 5.000 - 1.900 |
R-factor | 0.1531 |
R-free | 0.20590 |
Structure solution method | DIFFERENCE FOURIER |
Starting model (for MR) | 2spl |
RMSD bond length | 0.009 |
RMSD bond angle | 0.018 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHELXL-96 |
Refinement software | SHELXL-96 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.000 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.064 | 0.292 |
Number of reflections | 17289 | |
<I/σ(I)> | 26.4 | 5.5 |
Completeness [%] | 99.0 | 99.8 |
Redundancy | 4.2 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 9 | pH 9. |