1JBC
CONCANAVALIN A
Experimental procedure
| Source type | ROTATING ANODE |
| Source details | RIGAKU RUH2R |
| Temperature [K] | 120 |
| Detector technology | AREA DETECTOR |
| Collection date | 1994-08 |
| Detector | ADSC |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 61.954, 86.053, 89.079 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | ? - 1.150 |
| R-free | 0.16700 |
| Structure solution method | REFINEMENT |
| Starting model (for MR) | 3cna |
| RMSD bond length | 0.018 |
| RMSD bond angle | 0.193 |
| Phasing software | SHELXL-92 |
| Refinement software | SHELXL-92 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 1.250 | |
| High resolution limit [Å] | 1.150 | 1.150 |
| Rmerge | 0.042 | 0.019 |
| Number of reflections | 112810 | |
| <I/σ(I)> | 10.11 | |
| Completeness [%] | 83.8 | 73.6 |
| Redundancy | 3.5 | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | other * | Kalb, A.J., (1988) J. Crystal Growth, 88, 537. * |
