1JAC
A NOVEL MODE OF CARBOHYDRATE RECOGNITION IN JACALIN, A MORACEAE PLANT LECTIN WITH A BETA-PRISM
Experimental procedure
Source type | SEALED TUBE |
Detector technology | AREA DETECTOR |
Collection date | 1992 |
Detector | SIEMENS |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 129.600, 129.600, 157.900 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 2.430 |
R-factor | 0.174 |
Rwork | 0.174 |
R-free | 0.26000 |
RMSD bond length | 0.011 |
RMSD bond angle | 27.800 * |
Data reduction software | XENGEN |
Data scaling software | XENGEN |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.430 * |
Rmerge | 0.080 |
Total number of observations | 219402 * |
Number of reflections | 23791 |
Completeness [%] | 78.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 7.3 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 30 (mg/ml) | |
10 | 1 | reservoir | 0.05 (%(w/v)) | ||
11 | 1 | reservoir | methyl-alpha-D-galactopyranoside | 60 (M) | |
2 | 1 | drop | phosphate | 0.02 (M) | |
3 | 1 | drop | 0.1 (M) | ||
4 | 1 | drop | 0.05 (%(w/v)) | ||
5 | 1 | drop | methyl-alpha-D-galactopyranoside | 60 (M) | |
6 | 1 | drop | PEG4000 | 5-6 (%(w/v)) | |
7 | 1 | reservoir | PEG4000 | 40 (%) | |
8 | 1 | reservoir | phosphate | 0.02 (M) | |
9 | 1 | reservoir | 0.1 (M) |