1J52
Recombinant sperm whale myoglobin in the presence of 7atm xenon
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | SIEMENS |
Temperature [K] | 295 |
Detector technology | IMAGE PLATE |
Collection date | 1998-04-24 |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | P 6 |
Unit cell lengths | 91.580, 91.580, 45.970 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 5.000 - 1.900 |
Rwork | 0.155 |
R-free | 0.20500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1MBW |
RMSD bond length | 0.009 |
RMSD bond angle | 1.600 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 1.900 |
Rmerge | 0.067 |
Number of reflections | 16336 |
Completeness [%] | 93.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 9 | 2.6-3.0 M (NH4)2SO4, 20 mM TRIS, 1 mM EDTA, PH 9.0 |