1J52
Recombinant sperm whale myoglobin in the presence of 7atm xenon
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | SIEMENS |
| Temperature [K] | 295 |
| Detector technology | IMAGE PLATE |
| Collection date | 1998-04-24 |
| Detector | RIGAKU RAXIS IIC |
| Spacegroup name | P 6 |
| Unit cell lengths | 91.580, 91.580, 45.970 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 5.000 - 1.900 |
| Rwork | 0.155 |
| R-free | 0.20500 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1MBW |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.600 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Refinement software | X-PLOR (3.851) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.900 |
| Rmerge | 0.067 |
| Number of reflections | 16336 |
| Completeness [%] | 93.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 9 | 2.6-3.0 M (NH4)2SO4, 20 mM TRIS, 1 mM EDTA, PH 9.0 |
