1J48
Crystal Structure of Apo-C1027
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SRS BEAMLINE |
Synchrotron site | SRS |
Temperature [K] | 115 |
Detector technology | CCD |
Collection date | 2001-02-05 |
Detector | MARRESEARCH |
Spacegroup name | P 31 |
Unit cell lengths | 55.150, 55.150, 55.870 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 500.000 - 1.800 |
Rwork | 0.185 |
R-free | 0.23700 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.730 |
Data reduction software | DENZO (2000) |
Data scaling software | SCALEPACK (2000) |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.730 |
High resolution limit [Å] | 1.600 | 1.700 |
Rmerge | 0.076 | 0.650 |
Number of reflections | 41467 | |
<I/σ(I)> | 3 | |
Completeness [%] | 91.3 | 87.4 |
Redundancy | 2.3 | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | HANGING DROP/VAPOR DIFFUSION | 6.5 | 291 | Ammonium sulfate, Cacodylic acid, pH 6.5, HANGING DROP/VAPOR DIFFUSION, temperature 291.0K |