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1J48

Crystal Structure of Apo-C1027

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSRS BEAMLINE
Synchrotron siteSRS
Temperature [K]115
Detector technologyCCD
Collection date2001-02-05
DetectorMARRESEARCH
Spacegroup nameP 31
Unit cell lengths55.150, 55.150, 55.870
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution500.000 - 1.800
Rwork0.185
R-free0.23700
RMSD bond length0.014
RMSD bond angle1.730
Data reduction softwareDENZO (2000)
Data scaling softwareSCALEPACK (2000)
Refinement softwareCNS (1.0)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.730
High resolution limit [Å]1.6001.700
Rmerge0.0760.650
Number of reflections41467
<I/σ(I)>3
Completeness [%]91.387.4
Redundancy2.32
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1HANGING DROP/VAPOR DIFFUSION6.5291Ammonium sulfate, Cacodylic acid, pH 6.5, HANGING DROP/VAPOR DIFFUSION, temperature 291.0K

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