1J16

BENZAMIDINE IN COMPLEX WITH RAT TRYPSIN MUTANT X99/175/190RT

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	MPG/DESY, HAMBURG BEAMLINE BW6
Synchrotron site	MPG/DESY, HAMBURG
Beamline	BW6
Temperature [K]	100
Detector technology	CCD
Collection date	2000-04-04
Detector	ADSC QUANTUM 4
Wavelength(s)	0.95
Spacegroup name	I 2 3
Unit cell lengths	123.310, 123.310, 123.310
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 1.600
Rwork	0.189
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	18.180
High resolution limit [Å]	1.600
Number of reflections	40861

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7		pH 7.0