1J15

BENZAMIDINE IN COMPLEX WITH RAT TRYPSIN MUTANT X99/175/190RT

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU300
Temperature [K]	287
Detector technology	IMAGE PLATE
Collection date	2000-02-08
Detector	RIGAKU RAXIS IV
Wavelength(s)	1.5418
Spacegroup name	I 2 3
Unit cell lengths	124.700, 124.700, 124.700
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 2.000
Rwork	0.173
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	33.330
High resolution limit [Å]	2.000
Number of reflections	21903

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7		pH 7.0