1J14

BENZAMIDINE IN COMPLEX WITH RAT TRYPSIN MUTANT X99RT

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU300
Temperature [K]	287
Detector technology	IMAGE PLATE
Collection date	1998-06-04
Detector	RIGAKU RAXIS IV
Wavelength(s)	1.5418
Spacegroup name	I 2 3
Unit cell lengths	124.520, 124.520, 124.520
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 2.400
Rwork	0.193
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	50.840
High resolution limit [Å]	2.400
Number of reflections	12713

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		7		pH 7.0