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1IXV

Crystal Structure Analysis of homolog of oncoprotein gankyrin, an interactor of Rb and CDK4/6

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-18B
Synchrotron sitePhoton Factory
BeamlineBL-18B
Temperature [K]278
Detector technologyCCD
Collection date2002-01-22
DetectorADSC QUANTUM 4
Wavelength(s)1.0
Spacegroup nameP 21 21 21
Unit cell lengths41.433, 61.736, 98.095
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution30.000

*

- 2.300
Rwork0.194
R-free0.22900

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Structure solution methodMIR
RMSD bond length0.006
RMSD bond angle1.300
Data scaling softwareSCALA
Phasing softwareSOLVE
Refinement softwareCNS (1.0)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]30.0002.460
High resolution limit [Å]2.3002.300
Rmerge0.0850.216
Number of reflections11582
<I/σ(I)>6.63.2
Completeness [%]99.098.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.5298Adachi, N., (2002) Acta Cryst., D58, 859.

*

Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein5 (mg/ml)
21reservoirPEG400015-20 (%)
31reservoirMES0.1 (M)pH6.5

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