1IVB
STRUCTURES OF AROMATIC INHIBITORS OF INFLUENZA VIRUS NEURAMINIDASE
Experimental procedure
Spacegroup name | P 4 21 2 |
Unit cell lengths | 124.540, 124.540, 71.820 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.500 - 2.400 |
R-factor | 0.189 |
Rwork | 0.189 |
RMSD bond length | 0.016 |
RMSD bond angle | 2.142 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Rmerge | 0.104 * |
Number of reflections | 15271 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7.4 * | Lin, Y., (1990) J. Mol. Biol., 214, 639. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | PEG4000 | 10 (%(v/v)) | |
2 | 1 | drop | HEPES | 0.01 (M) | |
3 | 1 | drop | 10 (mM) | ||
4 | 1 | drop | 2.5 (mM) | ||
5 | 1 | reservoir | PEG4000 | 20 (%(v/v)) | |
6 | 1 | reservoir | HEPES | 0.02 (M) |