1IV5
New Crystal Form of Human CD81 Large Extracellular Loop.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL40B2 |
Synchrotron site | SPring-8 |
Beamline | BL40B2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2001-01-01 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.977 |
Spacegroup name | P 64 |
Unit cell lengths | 102.052, 102.052, 35.283 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 18.730 - 2.600 |
R-factor | 0.23376 |
Rwork | 0.229 |
R-free | 0.28220 |
RMSD bond length | 0.024 |
RMSD bond angle | 2.116 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | EPMR |
Refinement software | REFMAC (5.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.690 |
High resolution limit [Å] | 2.600 | 2.600 |
Rmerge | 0.050 | 0.206 |
Number of reflections | 32025 | |
Completeness [%] | 98.2 | 89 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 293 | PEG 4000, DMSO, sodium chloride, sodium acetate, pH 5.0, VAPOR DIFFUSION, SITTING DROP, temperature 293K |