1IUE
Crystal Structure Analysis of ferredoxin from Plasmodium falciparum
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2001-09-01 |
| Detector | RIGAKU RAXIS IV |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 49.000, 50.573, 52.480 |
| Unit cell angles | 90.00, 115.53, 90.00 |
Refinement procedure
| Resolution | 47.360 - 1.700 |
| R-factor | 0.184 |
| Rwork | 0.184 |
| R-free | 0.22100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.300 |
| Data reduction software | d*TREK |
| Data scaling software | d*TREK |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.360 | 1.760 |
| High resolution limit [Å] | 1.700 | 1.700 |
| Rmerge | 0.085 | 0.187 |
| <I/σ(I)> | 14.8 | 4.2 |
| Completeness [%] | 97 | |
| Redundancy | 3.48 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | PEG 8000, sodium acetate trihydrate, cacodylate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
