1IU7
HOLO FORM OF COPPER-CONTAINING AMINE OXIDASE FROM ARTHROBACTER GLOBIFORMIS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44B2 |
Synchrotron site | SPring-8 |
Beamline | BL44B2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 1999-10-04 |
Detector | MARRESEARCH |
Wavelength(s) | 0.7 |
Spacegroup name | I 1 2 1 |
Unit cell lengths | 157.794, 62.633, 183.956 |
Unit cell angles | 90.00, 111.74, 90.00 |
Refinement procedure
Resolution | 7.000 - 1.800 |
R-factor | 0.211 |
Rwork | 0.209 |
R-free | 0.25200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.841 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | X-PLOR |
Refinement software | X-PLOR (3.851) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.200 | 1.790 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.040 | |
Number of reflections | 172839 | |
Completeness [%] | 98.8 | 86.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | MICRODIALYSIS | 6.8 | 293 | potassium sodium tartrate, pH 6.8, MICRODIALYSIS, temperature 293K |