1IRC

CYSTEINE RICH INTESTINAL PROTEIN

Experimental procedure

Detector technology	AREA DETECTOR
Detector	XUONG-HAMLIN MULTIWIRE
Spacegroup name	P 21 21 21
Unit cell lengths	40.150, 49.040, 79.140
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 2.170
RMSD bond length	0.021 *
RMSD bond angle	2.900 *
Data reduction software	SDMS
Refinement software	TNT

Data quality characteristics

	Overall
Low resolution limit [Å]	26.600 *
High resolution limit [Å]	2.170 *
Rmerge	0.033
Total number of observations	25555 *
Number of reflections	7676
Completeness [%]	89.0
Redundancy	3.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	6.2 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG8000	35 (%)
2	1	reservoir		300 (mM)
3	1	reservoir	PIPES	0.1 (M)
4	1	reservoir	dioxane	0.1 (%)
5	1	drop	protein	6 (mg/ml)
6	1	drop	imidazole	5 (mM)