1IHP
STRUCTURE OF PHOSPHOMONOESTERASE
Experimental procedure
Source type | ROTATING ANODE |
Source details | OTHER |
Temperature [K] | 273 |
Detector technology | IMAGE PLATE |
Detector | MARRESEARCH |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 92.250, 92.250, 100.890 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.000 - 2.500 |
R-factor | 0.155 |
Rwork | 0.155 |
R-free | 0.21100 |
Structure solution method | SIRAS |
RMSD bond length | 0.009 |
RMSD bond angle | 22.800 * |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.600 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.056 * | |
Total number of observations | 79917 * | |
Number of reflections | 17223 | |
<I/σ(I)> | 28 | 7 |
Completeness [%] | 97.7 | 93.8 |
Redundancy | 4.6 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * |