Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Collection date | 1999-01-01 |
| Spacegroup name | P 4 21 2 |
| Unit cell lengths | 99.580, 99.580, 100.000 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 24.000 - 3.700 |
| R-factor | 0.361 |
| Rwork | 0.361 |
| R-free | 0.45800 |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 3.700 * |
| Total number of observations | 48037 * |
| Number of reflections | 19839 * |
| Completeness [%] | 63.0 * |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 7.2 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | protein | 1.0 (mg/ml) | |
| 2 | 1 | 1 | lipid | 0.28-0.33 (mg/ml) | |
| 3 | 1 | 1 | detergent | 70-120 (mM) | |
| 4 | 1 | 1 | 20 (mM) | ||
| 5 | 1 | 1 | 100 (mM) | ||
| 6 | 1 | 1 | EDTA | 0.1 (mM) | |
| 7 | 1 | 1 | 0.025 (%(w/v)) |
