1IGS
INDOLE-3-GLYCEROLPHOSPHATE SYNTHASE FROM SULFOLOBUS SOLFATARICUS AT 2.0 A RESOLUTION
Experimental procedure
Temperature [K] | 277 |
Detector technology | IMAGE PLATE |
Collection date | 1993-12-23 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 58.000, 73.800, 104.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 2.000 |
R-factor | 0.177 |
Rwork | 0.177 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.600 |
Data reduction software | MOSFLM |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 15.000 |
High resolution limit [Å] | 2.000 |
Rmerge | 0.073 |
Total number of observations | 205248 * |
Number of reflections | 29607 |
Completeness [%] | 96.0 |
Redundancy | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 5 | 4 * | pH 5. |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | potassium phosphate | 50 (mM) | |
2 | 1 | drop | EDTA | 5 (mM) | |
3 | 1 | drop | DTE | 2 (mM) | |
4 | 1 | drop | protein | 20 (mg/ml) | |
5 | 1 | reservoir | ammonium sulfate | 26-30 (%sat) |