1ICX
CRYSTAL STRUCTURE OF PATHOGENESIS-RELATED PROTEIN LLPR10.1A FROM YELLOW LUPINE
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | LURE BEAMLINE D41A |
Synchrotron site | LURE |
Beamline | D41A |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1999-07-17 |
Detector | MARRESEARCH |
Wavelength(s) | 1.3750 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 34.973, 56.617, 61.755 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 12.000 - 1.950 |
R-factor | 0.196 |
Rwork | 0.196 |
R-free | 0.25000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1btv |
RMSD bond length | 0.016 |
RMSD bond angle | 1.900 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (0.9) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 * | 2.020 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.053 | 0.127 |
Total number of observations | 89375 * | |
Number of reflections | 9446 | |
<I/σ(I)> | 25.73 | 8.46 |
Completeness [%] | 99.5 | 96.8 |
Redundancy | 9.5 * | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 292 | ammonium sulfate, TRIS, sucrose laureate, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 292K |