1ICN

ESCHERICHIA COLI-DERIVED RAT INTESTINAL FATTY ACID BINDING PROTEIN WITH BOUND MYRISTATE AT 1.5 A RESOLUTION AND I-FABPARG106-->GLN WITH BOUND OLEATE AT 1.74 A RESOLUTION

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	35.820, 51.550, 31.240
Unit cell angles	90.00, 92.28, 90.00

Refinement procedure

Resolution	? - 1.740
R-factor	0.161
RMSD bond length	0.010
RMSD bond angle	2.700
Phasing software	X-PLOR
Refinement software	TNT

Data quality characteristics

	Overall
Low resolution limit [Å]	10.000 *
High resolution limit [Å]	1.700 *
Rmerge	0.062 *
Total number of observations	21791 *
Number of reflections	10336 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	7.1 *	17 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	3.2 (mM)
2	1	reservoir	PEG8000	35-40 (%)
3	1	reservoir	PIPES	20 (mM)
4	1	reservoir	n-octylglucoside	0.1 (%(w/v))