1HYP

CRYSTAL STRUCTURE OF HYDROPHOBIC PROTEIN FROM SOYBEAN; A MEMBER OF A NEW CYSTINE-RICH FAMILY

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	52.100, 43.300, 28.600
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - 1.800
R-factor	0.187 *
Rwork	0.187
RMSD bond length	0.027
RMSD bond angle	4.200
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	1.800 *	1.800 *
Rmerge	0.038 *
Number of reflections	4943 *
Completeness [%]	78.0 *	72 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	ammonium sulfate	1.25 (M)
2	1	reservoir		2 (M)
3	1	reservoir	dioxane		0.100ml
4	1	drop	acetic acid	1.25 (M)
5	1	drop	protein	30 (mg/ml)
6	1	drop	octyl-beta-glucoside	0.1 (%(v/v))