1HXP

NUCLEOTIDE TRANSFERASE

Experimental procedure

Collection date	1993
Spacegroup name	P 21 21 2
Unit cell lengths	58.600, 217.200, 69.600
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	50.000 - 1.800
R-factor	0.191 *
RMSD bond length	0.018 *
RMSD bond angle	2.200 *
Data reduction software	DENZO
Data scaling software	XSCALIBRE
Refinement software	TNT

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	1.800 *	1.800 *
Rmerge	0.022 *	0.096 *
Total number of observations	169713 *
Number of reflections	68553 *	11827 *
Completeness [%]	82.0 *	70 *
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	5.9 *	277 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	17.5-23 (mg/ml)
2	1	reservoir	PEG10000	14.5 (%(v/v))
3	1	reservoir		400 (mM)
4	1	reservoir		250 (mM)
5	1	reservoir	phenyl-UDP	4 (mM)
6	1	reservoir		1 (mM)