1HXF
HUMAN THROMBIN COMPLEX WITH HIRUDIN VARIANT
Experimental procedure
Detector technology | AREA DETECTOR |
Collection date | 1996-02-20 |
Detector | SIEMENS |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 70.660, 72.470, 73.090 |
Unit cell angles | 90.00, 100.75, 90.00 |
Refinement procedure
Resolution | 7.000 - 2.300 * |
R-factor | 0.151 |
RMSD bond length | 0.014 |
RMSD bond angle | 0.049 |
Data reduction software | XENGEN |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.300 * |
Rmerge | 0.048 |
Total number of observations | 44309 * |
Number of reflections | 14047 * |
Completeness [%] | 91.0 * |
Redundancy | 2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 8.5 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | Tris | 0.1 (M) | |
2 | 1 | reservoir | PEG4000 | 28 (%) | |
3 | 1 | reservoir | sodium acetate | 0.2 (M) | |
4 | 1 | reservoir | 0.19 (M) |