1HSB

DIFFERENT LENGTH PEPTIDES BIND TO HLA-AW68 SIMILARLY AT THEIR ENDS BUT BULGE OUT IN THE MIDDLE

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	59.430, 78.469, 111.904
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	5.500 * - 1.900
R-factor	0.22
Rwork	0.220
RMSD bond length	0.017
RMSD bond angle	3.100
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	1.900 *
Rmerge	0.073 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *			referred to J.Mol.Biol. 186.205-210 1985 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	15 (mg/ml)
2	1	drop	2-(N-morpholino)ethanesulfonic acid	25 (mM)	can be replaced with 100mM imidazole
3	1	reservoir	PEG6000	15 (%(w/v))