1HLT

THE STRUCTURE OF A NONADECAPEPTIDE OF THE FIFTH EGF DOMAIN OF THROMBOMODULIN COMPLEXED WITH THROMBIN

Experimental procedure

Spacegroup name	P 43
Unit cell lengths	50.900, 50.900, 325.800
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 3.000
R-factor	0.146
Rwork	0.146
RMSD bond length	0.018
RMSD bond angle	0.048 *
Phasing software	X-PLOR
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	3.000 *
Rmerge	0.090 *
Number of reflections	12757 *
Completeness [%]	77.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	7.3 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG8000	26 (%)
2	1	reservoir	sodium phosphate	0.1 (M)
3	1	reservoir		1 (mM)