1HKL
FREE AND LIGANDED FORM OF AN ESTEROLYTIC CATALYTIC ANTIBODY
Experimental procedure
| Detector technology | IMAGE PLATE |
| Collection date | 1995 |
| Detector | RIGAKU |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 138.690, 44.490, 84.950 |
| Unit cell angles | 90.00, 121.75, 90.00 |
Refinement procedure
| Resolution | 6.000 - 2.700 * |
| R-factor | 0.184 |
| Rwork | 0.184 |
| R-free | 0.24400 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.536 |
| Data reduction software | DENZO |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 6.000 * |
| High resolution limit [Å] | 2.700 * |
| Rmerge | 0.143 |
| Number of reflections | 10159 |
| Completeness [%] | 80.9 |
| Redundancy | 2.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 7 * | 4 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | reservoir | sodium acetate | 100 (mM) | |
| 2 | 1 | reservoir | sodium cacodylate | 100 (mM) | |
| 3 | 1 | reservoir | PEG3300 | 27 (%(w/v)) |
