1HJE
Crystal structure of alpha-conotoxin SI
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SRS |
| Synchrotron site | SRS |
| Temperature [K] | 150 |
| Detector technology | CCD |
| Collection date | 2000-07-15 |
| Detector | BRUKER AXS |
| Spacegroup name | P 65 |
| Unit cell lengths | 32.092, 32.092, 14.669 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 10.910 - 0.750 |
| R-factor | 0.127 |
| Structure solution method | DIRECT METHODS |
| Data reduction software | SAINT |
| Data scaling software | SADABS |
| Phasing software | SHELX |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 10.910 | 0.870 |
| High resolution limit [Å] | 0.750 | 0.750 |
| Number of reflections | 21312 | |
| <I/σ(I)> | 19.65 | 2.07 |
| Completeness [%] | 97.9 | 96.3 |
| Redundancy | 5.99 | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 0.4M K,NA TARTRATE |
