1HBQ
CRYSTAL STRUCTURE OF LIGANDED AND UNLIGANDED FORMS OF BOVINE PLASMA RETINOL-BINDING PROTEIN
Experimental procedure
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.550, 48.970, 76.870 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 9.000 * - 1.700 |
R-factor | 0.196 |
Rwork | 0.196 |
RMSD bond length | 0.011 |
RMSD bond angle | 2.900 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 2.700 * |
High resolution limit [Å] | 2.200 * |
Rmerge | 0.059 * |
Total number of observations | 70544 * |
Number of reflections | 18382 * |
Completeness [%] | 94.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Microdialysis * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | bRBP | 6-10 (mg/ml) | |
2 | 1 | 2 | sodium chloride | 0.1 (M) | |
3 | 1 | 2 | cadmium acetate | 0.01-1. (mM) | |
4 | 1 | 2 | sodium acetate | 0.1 (M) |