1HBB
HIGH-RESOLUTION X-RAY STUDY OF DEOXYHEMOGLOBIN ROTHSCHILD 37BETA TRP-> ARG: A MUTATION THAT CREATES AN INTERSUBUNIT CHLORIDE-BINDING SITE
Experimental procedure
Spacegroup name | P 21 21 2 |
Unit cell lengths | 97.000, 99.300, 66.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 * - 1.900 |
R-factor | 0.185 |
RMSD bond length | 0.010 |
RMSD bond angle | 0.024 |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.910 * |
Rmerge | 0.044 * |
Total number of observations | 18175 * |
Number of reflections | 47999 * |
Completeness [%] | 95.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Batch method * | 7 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | hemoglobin | 10 (mg/ml) | |
2 | 1 | 1 | potassium phosphate | 10 (mM) | |
3 | 1 | 1 | potassium chloride | 100 (mM) | |
4 | 1 | 1 | sodium dithionite | 4 (mM) | |
5 | 1 | 1 | PEG6000 | 10-10.5 (%) |