1H9V
Human Fc-gamma-Receptor IIa (FcgRIIa), monoclinic
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 291 |
Detector technology | IMAGE PLATE |
Collection date | 2000-03-15 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 81.310, 50.000, 55.450 |
Unit cell angles | 90.00, 128.30, 90.00 |
Refinement procedure
Resolution | 50.000 * - 3.000 |
R-factor | 0.246 * |
R-free | 0.32700 * |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2fcb |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | |
High resolution limit [Å] | 3.000 | |
Rmerge | 0.111 * | 0.242 * |
Number of reflections | 3417 | |
Completeness [%] | 90.5 | 69 * |
Redundancy | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, sitting drop * | 7.2 * | 20 * | 0.2M NAOAC PH 4.6, 26% PEG 8000 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | MOPS | 2 (mM) | |
2 | 1 | drop | 150 (mM) | ||
3 | 1 | drop | sodium azide | 0.02 (%) | |
4 | 1 | reservoir | sodium acetate/acetic acid | 0.2 (M) | |
5 | 1 | reservoir | PEG8000 | 26 (%) |