1H9H
COMPLEX OF EETI-II WITH PORCINE TRYPSIN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 1999-04-04 |
Detector | MARRESEARCH |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 121.050, 121.050, 121.050 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.500 |
R-factor | 0.2331 |
R-free | 0.27580 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ldt |
RMSD bond length | 0.009 |
RMSD bond angle | 0.028 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.600 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.053 | 0.376 |
Number of reflections | 49533 | |
<I/σ(I)> | 19.24 | 3.39 |
Completeness [%] | 99.7 | 99.6 |
Redundancy | 8.05 | 4.48 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.7 | pH 6.70 |