1H9H

COMPLEX OF EETI-II WITH PORCINE TRYPSIN

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID14-2
Synchrotron site	ESRF
Beamline	ID14-2
Temperature [K]	100
Detector technology	CCD
Collection date	1999-04-04
Detector	MARRESEARCH
Spacegroup name	P 41 3 2
Unit cell lengths	121.050, 121.050, 121.050
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 - 1.500
R-factor	0.2331
R-free	0.27580
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1ldt
RMSD bond length	0.009
RMSD bond angle	0.028
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	AMoRE
Refinement software	SHELXL-97

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	1.600
High resolution limit [Å]	1.500	1.500
Rmerge	0.053	0.376
Number of reflections	49533
<I/σ(I)>	19.24	3.39
Completeness [%]	99.7	99.6
Redundancy	8.05	4.48

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		6.7		pH 6.70