1H7U
hPMS2-ATPgS
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2001-02-15 |
Detector | RIGAKU RAXIS IV |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 74.357, 73.868, 136.120 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.450 - 2.700 |
R-factor | 0.237 |
Rwork | 0.237 |
R-free | 0.27000 |
Structure solution method | OTHER |
RMSD bond length | 0.010 |
RMSD bond angle | 1.800 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (0.9) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 2.800 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.061 | 0.362 |
Number of reflections | 20269 | |
<I/σ(I)> | 14.5 | 1.8 |
Completeness [%] | 95.1 | 89.3 |
Redundancy | 2.7 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6.2 | 2-2.4 M NA/K PHOSPHATE (PH=6.2) 0.2 M LICL, pH 6.20 |