1GWF

Compound II structure of Micrococcus Lysodeikticus catalase

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU
Temperature [K]	120
Detector technology	IMAGE PLATE
Collection date	1995-10-15
Detector	MARRESEARCH
Spacegroup name	P 42 21 2
Unit cell lengths	106.190, 106.190, 105.300
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	74.540 - 1.960
R-factor	0.08935
Rwork	0.141
R-free	0.18966
Structure solution method	OTHER
Data reduction software	DENZO
Data scaling software	SCALEPACK
Refinement software	REFMAC (5)

Data quality characteristics

	Overall
Low resolution limit [Å]	74.536
High resolution limit [Å]	1.936
Rmerge	0.061
Number of reflections	41376
<I/σ(I)>	8
Completeness [%]	99.5
Redundancy	5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		5.2		pH 5.20